Guest guest Posted November 13, 2011 Report Share Posted November 13, 2011 > > Hi everyone! > > The other day I wanted to make solid perfume with vanilla and some citruses and everything was good until I poured mix into jar and entire vanilla sank down. > Vanilla can be a rough one, that's for sure, due to what seem to be various sugars and more solid matter that either aren't soluble in one thing while the rest of the vanilla is, to say nothing of what appears to be density differences....I've had the same thing happen. One trick is to let the stuff harden to a certain extent then stir it up so its all mixed again, just not as completely of course but close enough. This is all amateur trail and error mind you, and I'm betting there are some classes out there which would be very helpful if you are wanting some professional expertise with making solid perfumes...keep me posted if you figure it out, please! M. > Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 13, 2011 Report Share Posted November 13, 2011 > > Hi everyone! > > The other day I wanted to make solid perfume with vanilla and some citruses and everything was good until I poured mix into jar and entire vanilla sank down. > **************************** Vanilla can be tricky like that. I think vanilla absolute is the worst of the vanillas for soluability in oils. Vanilla CO2 seems to blend better into oils in my experience, but the scent is definitely different from vanilla absolutes. Vanilla absolute won't likely dissolve completely, but folks here in the group have reported pretty decent results with letting the vanilla absolute sit in the oil for a few months, with occasional shaking, and the scent infuses well into the oil. Then you just filter out the undissolved parts or carefully decant the infused oil off so you don't have solids left over in your final product. If you do a search in the message archives, there has been some discussion on the process and results. Best of luck, Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 13, 2011 Report Share Posted November 13, 2011  Hi everyone! The other day I wanted to make solid perfume with vanilla and some citruses and everything was good until I poured mix into jar and entire vanilla sank down. All my ingredients are 100% natural, no fake stuff inside. I have no idea how to deal with this. Thank you for your help. What form of vanilla are you using? A good solution might be to make a vanilla infusion to use as your base liquid oil.  Soak a vanilla bean in a couple ounces of jojoba or coconut oil(vanilla in virgin coconut oil is heavenly). Let sit a couple to a few weeks. You can strain it out or just keep the bean in the oil(that's what I do-I'm too lazy).   At first I wanted to say that this has never happened to me, and then I realized that I've never made a solid perfume with vanilla! Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 Hi , I used vanilla absolute. Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 > Vanilla can be tricky like that. I think vanilla absolute is the worst of the vanillas for soluability in oils. Vanilla CO2 seems to blend better into oils in my experience, but the scent is definitely different from vanilla absolutes. Vanilla absolute won't likely dissolve completely, but folks here in the group have reported pretty decent results with letting the vanilla absolute sit in the oil for a few months, with occasional shaking, and the scent infuses well into the oil. Then you just filter out the undissolved parts or carefully decant the infused oil off so you don't have solids left over in your final product. If you do a search in the message archives, there has been some discussion on the process and results. > > Best of luck, > I could do it like that but I always fear that I might not be able to repeat it identically... that it will dissolve differently... Any quality sources for Vanilla CO2? Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 Hi Ankica/, Try using vanilla Co2 instead of the absolute. Â I use this in my solids and I have never had a problem with the vanilla sinking to the bottom or separating. Â I like Eden Botanicals vanilla co2, it's good and strong and you can get away with using a little less as it has a high vanillin content. Best, Charna Ethier Providence Perfume Co. http://www.providenceperfume.com info@... Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 Thanks Charna, I will. There was also one more thing... On the bottom of the jar - the liquid was thinner. Like 3 water drops were captured. Any clue why is that? Ankica bellatrixperfumes.com Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 > > Hi everyone! > > The other day I wanted to make solid perfume with vanilla and some citruses and everything was good until I poured mix into jar and entire vanilla sank down. > (sorry for the double message, it went out of webmail without a subject) I can't say that I've ever had that problem, but I work the oils into the heated base, and keep stirring as I pour. The woman who taught me to make solid perfumes said to put a drop of the perfume on the top of the solid base so it has an extra push. This may help. Alwyn L'hoir www.BlueMoonPerfume.com Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 >The other day I wanted to make solid perfume with vanilla and some citruses and everything was good until I poured mix into jar and entire vanilla sank down. If it is absolute, try cutting it with a little fractionated coconut oil before mixing it into your base. Cat Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 > > Hi , > > I used vanilla absolute._______________________________- I have had the same experience~ It appears that vanilla absolute does not dissolve in oil You can use this extraction in alcohol based perfumes. s idea works great as well as using a CO2 extraction. Ragna > Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011  Hi Ankica/, Try using vanilla Co2 instead of the absolute.  I use this in my solids and I have never had a problem with the vanilla sinking to the bottom or separating.  I like Eden Botanicals vanilla co2, it's good and strong and you can get away with using a little less as it has a high vanillin content. Best, Charna Ethier Providence Perfume Co. http://www.providenceperfume.com info@... Hi Charna I have that Co2 as well as the absolute. It's nice, but it's funny, to me the CO2 is the lighter one. Maybe it's the batch I have.  I also like that the color is light. Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 ________________________________ > ****************************  Vanilla can be tricky like that. I think vanilla absolute is the worst of the vanillas for soluability in oils. Vanilla CO2 seems to blend better into oils in my experience, but the scent is definitely different from vanilla absolutes. Vanilla absolute won't likely dissolve completely, but folks here in the group have reported pretty decent results with letting the vanilla absolute sit in the oil for a few months, with occasional shaking, and the scent infuses well into the oil. Then you just filter out the undissolved parts or carefully decant the infused oil off so you don't have solids left over in your final product. If you do a search in the message archives, there has been some discussion on the process and results.  Best of luck, That's one of the reasons I use alcohol!  There are so many essences that won't dissolve in oil. True, there are some that don't dissolve(or dissolve completely) in alcohol, but most essences do. Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 Thanks everybody! I will put vanilla abs in jojoba and I will buy co2. My biggest fear is that I won't be able to replicate perfume entirely - all these dilutions and thick materials which I need to take out from the bottle... every time something goes wrong... and final products smells different although I have entire formula written... on the bright side:I must say that I am overwhelmed by the beauty of osmanthus. It was in my last order from aroma-zone.com and it is great. And Ambrette from the same source... amazing! A. Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 Have you tried mixing all the essential oils you are using before blending them into the oil base? When I have solubility issues with thick aromatics I always blend them with the other more volatile essences and let them macerate for some time. There is much less residue afterwards. Mind you, this method doesn't work as well with alcohol based perfume. Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 14, 2011 Report Share Posted November 14, 2011 Thanks everybody! I will put vanilla abs in jojoba and I will buy co2. My biggest fear is that I won't be able to replicate perfume entirely - all these dilutions and thick materials which I need to take out from the bottle... every time something goes wrong... and final products smells different although I have entire formula written... *************** Hi Ankica, That is a challenge that every perfumer faces, and the short answer is there is going to be variation in your scent from batch to batch. Sometimes an oil or absolute will vary from batch to batch, supplier to supplier, region to region, year to year, etc. So anytime you buy a new aromatic, you may have to slightly tweak your formulas to get them as close to previous batches as you can, even if you used the exact same formulas. If you are letting the vanilla absolute sit in the carrier oil for a similar amount of time and in the same quantities, keeping things like the temperature you are keeping it in and how often you are shaking the bottle, it should turn out reasonable similar in vanilla odor and strength from batch to batch. And if you notice a bit of difference, then you modify as needed. The idea of trying to mix in a bit of fractionated coconut oil first sounds promising, I would definitely give that a try. Thanks Cat! Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 15, 2011 Report Share Posted November 15, 2011 > > Have you tried mixing all the essential oils you are using before blending them into the oil base? When I have solubility issues with thick aromatics I always blend them with the other more volatile essences and let them macerate for some time. There is much less residue afterwards. Mind you, this method doesn't work as well with alcohol based perfume. > Yes. But very soon I added jojoba. Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 15, 2011 Report Share Posted November 15, 2011 > What form of vanilla are you using? A good solution might be to make a vanilla infusion to use as your base liquid oil.  Soak a vanilla bean in a couple ounces of jojoba or coconut oil(vanilla in virgin coconut oil is heavenly). Let sit a couple to a few weeks. You can strain it out or just keep the bean in the oil(that's what I do-I'm too lazy).   At first I wanted to say that this has never happened to me, and then I realized that I've never made a solid perfume with vanilla! > > , are you keeping the vanilla in a warm spot to keep it liquid while its infusing? Quote Link to comment Share on other sites More sharing options...
Guest guest Posted November 15, 2011 Report Share Posted November 15, 2011 ________________________________  , are you keeping the vanilla in a warm spot to keep it liquid while its infusing?I live in Miami, so yes!  I just keep it in my cupboard. I don't know about the temperatures in your house but I would suggest a warm place if you were going to do that now. We had temperatures in the low 70's last week(sort of chilly for here) and the oil solidified as virgin coconut will do, but it is liquid again. It's been infusing since June I believe. The scent is rather light, I'm thinking of adding some more bean. I wanted to make a solid perfume with it, but I need the containers to put it in. I want to base it on flowers used in leis; frangipani, jasmine sambac (pikake), white ginger, and tuberose, on a Tahitian vanilla andVanuatu sandalwood base. I want to call it Gettin' Lei'd! Quote Link to comment Share on other sites More sharing options...
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